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8PhenomenexlEメール:jpinfo@phenomenex.comlWEB:www.phenomenex.com食品中カンナビノイド(GC-MS)ペットフード中メラミン(GC-MS)ExtractionProtocol:1.Combine1gofchocolatebrowniewith10mLofwaterina50mLcentrifugetube2.Shakeusingamechanicalshakeruntildissolved3.AddroQ™QuEChERSEN15662extractionsaltpacket(KS0-8909)and10mLofacetonitrile4.Shaketubefor3minusingmechanicalshaker5.Centrifugeat2700rpmfor5min6.Transfer1mLofsupernatanttoanautosamplervialforGC-MSanalysisColumn:Zebron™ZB-5MSPLUS™Dimensions:30meterx0.25 mmx0.25 µmPartNo.:7HG-G030-11Injection:Splitless@250°C,1µLCarrierGas:Helium@1.5mL/min(constantflow)OvenProgram:100°Cfor1minto320°C@50°C/minholdfor2minDetector:MSD@320°CSample: 1.Cannabidiol2.∆-9-Tetrahydrocannabinol3.Cannabinol AppID23244マトリックス抽出物の良好なピーク形状232441234591011121314minAppID2324591011121314min2324512345TICofspikeddogfood(100μg/g)TICofspikedbrownies(1μg/g)EICoftargetanalytesmin5.255.505.756.006.256.506.7512323229ExtractionProtocol:1.Combine0.5gofhomogenizeddogfoodwith10mLofDEA/Water/Acetonitrile(1:4:5)ina15mLcentrifugetube2.Sonicatefor30min3.Centrifugeat5000rpmfor10min4.Transfer100µLofsupernatanttoanautosamplervialandevaporatetodrynessusingnitrogengas5.Reconstitutewith100µLofAcetonitrile/Pyridine(1:1)andthenderivatizeusing100µLBSTFAwith1%TCMSat70°Cfor45minColumn:ZebronZebronZB-5MSPLUSDimensions:30meterx0.25 mmx0.25 µmPartNo.:7HG-G030-11Injection:Splitless@280°C,1µLCarrierGas:Helium@1mL/min(constantflow)OvenProgram:75°Cfor1minto320°C@15°C/minholdfor4minDetector:MSD@320°CSample: 1.Cyanuricacid2.Ammelide3.Ammeline4.Melamine5.Benzoguanamine AppID23229
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9PhenomenexlEメール:jpinfo@phenomenex.comlWEB:www.phenomenex.com乱用薬物(GC-MS)エタノールアミン(GC-MS)Column:ZebronZB-5MSPLUSDimensions:30meterx0.25 mmx1.00µmPartNo.:7HG-G030-22Injection:Split200:1@250°C,1µLCarrierGas:Helium@1.4mL/min(constantflow)OvenProgram:30°Cto300°C@40°C/minDetector:MSD@320°CSample: 1.Monoethanolamine2.Diethanolamine3.Triethyleneglycolmonomethylether(IS)4.Triethanolamine 良好なピーク形状AppID23246min21243345623246Column:Zebron™ZB-5MSPLUS™Dimensions:30meterx0.25 mmx0.25 µmPartNo.:7HG-G030-11Injection:Splitless@250°C,1µLCarrierGas:Helium@1.4 mL/min(constantflow)OvenProgram:70°Cfor1minto150°C@30°C/minto320°C@10°C/minfor5.5minDetector:MSD@250°C;45–450amuNote:Analytesare25 ppminMethanolSample: 1.Nicotine2.MDA3.MDMA4.MBDB5.Meperidine6.Benzamphetamine7.Glutethimide8.PCP9.Doxylamine10.Tramadol11.Procaine 12.Methadone13.Topiramate14.Cocaine15.Cocaethylene16.CBD17.Codeine18.Ethylmorphine19.Diazepam20.Hydrocodone21.Δ-9-Tetrahydrocannabinol22.6-MAM23.Oxycodone1234567891011121314151617222318-2145678910111213141516171819min1615.518192021AppID23258
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